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1. WO2020133022 - CYPYRAFLUONE DIMETHYLAMINE SALT, PREPARATION METHOD THEREFOR AND USE THEREOF

Publication Number WO/2020/133022
Publication Date 02.07.2020
International Application No. PCT/CN2018/124130
International Filing Date 27.12.2018
IPC
C07D 401/10 2006.01
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
DHETEROCYCLIC COMPOUNDS
401Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
02containing two hetero rings
10linked by a carbon chain containing aromatic rings
A01N 43/56 2006.01
AHUMAN NECESSITIES
01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
43Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
48having rings with two nitrogen atoms as the only ring hetero atoms
561,2-Diazoles; Hydrogenated 1,2-diazoles
C07C 211/04 2006.01
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
CACYCLIC OR CARBOCYCLIC COMPOUNDS
211Compounds containing amino groups bound to a carbon skeleton
01having amino groups bound to acyclic carbon atoms
02of an acyclic saturated carbon skeleton
03Monoamines
04Mono-, di- or tri-methylamine
C07C 209/00 2006.01
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
CACYCLIC OR CARBOCYCLIC COMPOUNDS
209Preparation of compounds containing amino groups bound to a carbon skeleton
A01P 13/00 2006.01
AHUMAN NECESSITIES
01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
PBIOCIDAL, PEST REPELLANT, PEST ATTRACTANT OR PLANT GROWTH REGULATORY ACTIVITY OF CHEMICAL COMPOUNDS OR PREPARATIONS
13Herbicides; Algicides
CPC
A01N 43/56
AHUMAN NECESSITIES
01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES, AS HERBICIDES
43Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
48having rings with two nitrogen atoms as the only ring hetero atoms
561,2-Diazoles; Hydrogenated 1,2-diazoles
C07C 209/00
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
CACYCLIC OR CARBOCYCLIC COMPOUNDS
209Preparation of compounds containing amino groups bound to a carbon skeleton
C07C 211/04
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
CACYCLIC OR CARBOCYCLIC COMPOUNDS
211Compounds containing amino groups bound to a carbon skeleton
01having amino groups bound to acyclic carbon atoms
02of an acyclic saturated carbon skeleton
03Monoamines
04Mono-, di- or tri-methylamine
C07D 401/10
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
DHETEROCYCLIC COMPOUNDS
401Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
02containing two hetero rings
10linked by a carbon chain containing aromatic rings
Applicants
  • 青岛清原化合物有限公司 QINGDAO KINGAGROOT CHEMICAL COMPOUND CO., LTD. [CN]/[CN]
Inventors
  • 连磊 LIAN, Lei
  • 赵德 ZHAO, De
  • 彭学岗 PENG, Xuegang
  • 金涛 JIN, Tao
Priority Data
201811593040.625.12.2018CN
Publication Language Chinese (ZH)
Filing Language Chinese (ZH)
Designated States
Title
(EN) CYPYRAFLUONE DIMETHYLAMINE SALT, PREPARATION METHOD THEREFOR AND USE THEREOF
(FR) SEL DE CYPYRAFLUONE DIMÉTHYLAMINE, SON PROCÉDÉ DE PRÉPARATION ET SON UTILISATION
(ZH) 环吡氟草酮二甲胺盐及其制备方法和用途
Abstract
(EN)
The present invention relates to a Cypyrafluone dimethylamine salt, a preparation method therefor, and use thereof. The present invention specifically relates to a crystal form A of the Cypyrafluone dimethylamine salt, and the X-ray powder diffraction spectrum has characteristic peaks at diffraction angles 2θ of 6.6°, 9.5°, 10.4°, 12.5°, 12.9°, 13.2°, 15.0°, 15.5°, 16.1°, 16.4°, 16.8°, 18.3°, 19.0°, 19.8°, 20.5°, 22.3°, 23.8°, 24.3°, 25.5°, 25.9°, 26.8°, 27.5°, 28.5°, 28.9°, 29.6°, 30.8°, 32.0°, 33.2°, 34.6°, 35.8°, 36.8°, 37.2°, 38.5°, 40.1°, 41.0°, 41.6°, and 42.4°, wherein the 2θ error range is within ±0.2°. The Cypyrafluone dimethylamine salt has good physical and chemical stability, high solubility and high bioactivity, and can be used for preventing common weeds in wheat fields.
(FR)
La présente invention concerne un sel de cypyrafluone diméthylamine, son procédé de préparation et son utilisation. La présente invention concerne en particulier une forme cristalline A du sel de cypyrafluone diméthylamine, et le spectre de diffraction de rayons X sur poudre a des pics caractéristiques à des angles de diffraction 2θ de 6,6°, 9,5°, 10,4°, 12,5°, 12,9°, 13,2°, 15,0°, 15,5°, 16,1°, 16,4°, 16,8°, 18,3°, 19,0°, 19,8°, 20,5°, 22,3°, 23,8°, 24,3°, 25,5°, 25,9°, 26,8°, 27,5°, 28,5°, 28,9°, 29,6°, 30,8°, 32,0°, 33,2°, 34,6°, 35,8°, 36,8°, 37,2°, 38,5°, 40,1°, 41,0°, 41,6° et 42,4°, la plage d'erreur 2θ étant de ± 0,2°. Le sel de cypyrafluone diméthylamine a une bonne stabilité physico-chimique, une solubilité élevée et une grande bioactivité, et peut être utilisé pour prévenir des mauvaises herbes communes dans des champs de blé.
(ZH)
涉及一种环吡氟草酮二甲胺盐及其制备方法和用途,具体涉及环吡氟草酮二甲胺盐A晶型,其X-射线粉末衍射谱图在衍射角2θ为6.6°、9.5°、10.4°、12.5°、12.9°、13.2°、15.0°、15.5°、16.1°、16.4°、16.8°、18.3°、19.0°、19.8°、20.5°、22.3°、23.8°、24.3°、25.5°、25.9°、26.8°、27.5°、28.5°、28.9°、29.6°、30.8°、32.0°、33.2°、34.6°、35.8°、36.8°、37.2°、38.5°、40.1°、41.0°、41.6°、42.4°处具有特征峰,其中2θ误差范围在±0.2°内。所述环吡氟草酮二甲胺盐物理化学稳定性好,溶解度大,生物活性较高,可用于小麦田常见杂草的防除。
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