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1. WO2020133015 - CYPYRAFLUONE MONOISOPROPYLAMINE SALT D CRYSTAL FORM, PREPARATION METHOD THEREFOR AND USE THEREOF

Publication Number WO/2020/133015
Publication Date 02.07.2020
International Application No. PCT/CN2018/124123
International Filing Date 27.12.2018
IPC
C07D 403/10 2006.01
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
DHETEROCYCLIC COMPOUNDS
403Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, not provided for by group C07D401/167
02containing two hetero rings
10linked by a carbon chain containing aromatic rings
C07D 227/087 2006.01
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
DHETEROCYCLIC COMPOUNDS
227Heterocyclic compounds containing rings having one nitrogen atom as the only ring hetero atom, according to more than one of groups C07D203/-C07D225/184
02with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
06with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
08Oxygen atoms
087One doubly-bound oxygen atom in position 2, e.g. lactams
C07D 229/02 2006.01
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
DHETEROCYCLIC COMPOUNDS
229Heterocyclic compounds containing rings of less than five members having two nitrogen atoms as the only ring hetero atoms
02containing three-membered rings
A01N 43/56 2006.01
AHUMAN NECESSITIES
01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
43Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
48having rings with two nitrogen atoms as the only ring hetero atoms
561,2-Diazoles; Hydrogenated 1,2-diazoles
A01N 43/84 2006.01
AHUMAN NECESSITIES
01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
43Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
72having rings with nitrogen atoms and oxygen or sulfur atoms, as ring hetero atoms
84six-membered rings with one nitrogen atom and either one oxygen atom or one sulfur atom in positions 1,4
A01N 43/60 2006.01
AHUMAN NECESSITIES
01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
43Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
48having rings with two nitrogen atoms as the only ring hetero atoms
601,4-Diazines; Hydrogenated 1,4-diazines
CPC
A01N 33/18
AHUMAN NECESSITIES
01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES, AS HERBICIDES
33Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
16containing nitrogen-to-oxygen bonds
18Nitro compounds
A01N 37/22
AHUMAN NECESSITIES
01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES, AS HERBICIDES
37Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
18containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof
22the nitrogen atom being directly attached to an aromatic ring system, e.g. anilides
A01N 37/40
AHUMAN NECESSITIES
01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES, AS HERBICIDES
37Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
36containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
38having at least one oxygen or sulfur atom attached to an aromatic ring system
40having at least one carboxylic group or a thio analogue, or a derivative thereof, and one oxygen or sulfur atom attached to the same aromatic ring system
A01N 39/04
AHUMAN NECESSITIES
01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES, AS HERBICIDES
39Biocides, pest repellants or attractants, or plant growth regulators containing aryloxy- or arylthio-aliphatic or cycloaliphatic compounds, containing the group or , e.g. phenoxyethylamine, phenylthio-acetonitrile, phenoxyacetone
02Aryloxy-carboxylic acids; Derivatives thereof
04Aryloxy-acetic acids; Derivatives thereof
A01N 43/40
AHUMAN NECESSITIES
01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES, AS HERBICIDES
43Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
34having rings with one nitrogen atom as the only ring hetero atom
40six-membered rings
A01N 43/54
AHUMAN NECESSITIES
01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES, AS HERBICIDES
43Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
48having rings with two nitrogen atoms as the only ring hetero atoms
541,3-Diazines; Hydrogenated 1,3-diazines
Applicants
  • 青岛清原化合物有限公司 QINGDAO KINGAGROOT CHEMICAL COMPOUND CO., LTD. [CN]/[CN]
Inventors
  • 连磊 LIAN, Lei
  • 赵德 ZHAO, De
  • 彭学岗 PENG, Xuegang
  • 金涛 JIN, Tao
Priority Data
201811592569.625.12.2018CN
Publication Language Chinese (ZH)
Filing Language Chinese (ZH)
Designated States
Title
(EN) CYPYRAFLUONE MONOISOPROPYLAMINE SALT D CRYSTAL FORM, PREPARATION METHOD THEREFOR AND USE THEREOF
(FR) FORME CRISTALLINE D D'UN SEL DE CYPYRAFLUONE MONOISOPROPYLAMINE, PROCÉDÉ DE PRÉPARATION CORRESPONDANT ET UTILISATION ASSOCIÉE
(ZH) 环吡氟草酮一异丙胺盐D晶型及其制备方法和用途
Abstract
(EN)
The present invention belongs to the technical field of herbicide crystallization processes, and specifically relates to a cypyrafluone monoisopropylamine salt D crystal form, a preparation method therefor and the use thereof. The X-ray powder diffraction spectrum of the cypyrafluone monoisopropylamine salt D crystal form has characteristic peaks at diffraction angle 2θ of 7.0º, 8.8º, 10.6º, 12.4º, 12.7º, 13.8º, 14.2º, 15.2º, 15.9º, 16.5º, 17.2º, 17.8º, 18.8º, 19.7º, 20.5º, 21.6º, 22.6º, 23.2º, 24.1º, 25.1º, 25.6º, 26.2º, 27.2º, 28.2º, 28.9º, 29.3º, 29.8º, 30.9º, 31.7º, 32.3º, 33.2º, 34.0º, 34.8º, 35.3º, 35.8º, 36.2º, 37.1º, 38.1º, 38.8º, 39.9º, 40.5º, 42.2º, and 42.6º, with a 2θ error range within ± 0.2º. The cypyrafluone monoisopropylamine salt D crystal form of the present invention has a good physicochemical stability, a high solubility and a high biological activity, and can be used for preventing and removing weeds.
(FR)
La présente invention se rapporte au domaine technique des procédés de cristallisation d'herbicides et concerne en particulier une forme cristalline D d'un sel de cypyrafluone monoisopropylamine, un procédé de préparation correspondant et une utilisation associée. Le spectre de diffraction de rayons X sur poudre de la forme cristalline D du sel de cypyrafluone monoisopropylamine présente des pics caractéristiques à un angle de diffraction 2θ de 7,0º, 8,8º, 10,6º, 12,4º, 12,7º, 13,8º, 14,2º, 15,2º, 15,9º, 16,5º, 17,2º, 17,8º, 18,8º, 19,7º, 20,5º, 21,6º, 22,6º, 23,2º, 24,1º, 25,1º, 25,6º, 26,2º, 27,2º, 28,2º, 28,9º, 29,3º, 29,8º, 30,9º, 31,7º, 32,3º, 33,2º, 34,0º, 34,8º, 35,3º, 35,8º, 36,2º, 37,1º, 38,1º, 38,8º, 39,9º, 40,5º, 42,2º et 42.6º, avec une plage d'erreurs 2θ de ± 0,2º. La forme cristalline D du sel de cypyrafluone monoisopropylamine selon la présente invention a une bonne stabilité physico-chimique, une solubilité élevée et une haute activité biologique, et peut être utilisée pour prévenir et éliminer des mauvaises herbes.
(ZH)
本发明属于除草剂结晶工艺技术领域,具体涉及一种环吡氟草酮一异丙胺盐D晶型及其制备方法和用途。所述环吡氟草酮一异丙胺盐D晶型的X-射线粉末衍射谱图在衍射角2θ为7.0°、8.8°、10.6°、12.4°、12.7°、13.8°、14.2°、15.2°、15.9°、16.5°、17.2°、17.8°、18.8°、19.7°、20.5°、21.6°、22.6°、23.2°、24.1°、25.1°、25.6°、26.2°、27.2°、28.2°、28.9°、29.3°、29.8°、30.9°、31.7°、32.3°、33.2°、34.0°、34.8°、35.3°、35.8°、36.2°、37.1°、38.1°、38.8°、39.9°、40.5°、42.2°、42.6°处具有特征峰,其中2θ误差范围在±0.2°内。本发明的环吡氟草酮一异丙胺盐D晶型物理化学稳定性好,溶解度大,生物活性较高,可用于防除杂草。
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