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1. WO2019037743 - STARCH-CONTAINING MICROSPHERE AND PREPARATION METHOD THEREFOR AND APPLICATION THEREOF

Publication Number WO/2019/037743
Publication Date 28.02.2019
International Application No. PCT/CN2018/101771
International Filing Date 22.08.2018
IPC
C08B 31/00 2006.1
CCHEMISTRY; METALLURGY
08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
BPOLYSACCHARIDES; DERIVATIVES THEREOF
31Preparation of chemical derivatives of starch
C08F 251/00 2006.1
CCHEMISTRY; METALLURGY
08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
251Macromolecular compounds obtained by polymerising monomers on to polysaccharides or derivatives thereof
C09K 8/514 2006.1
CCHEMISTRY; METALLURGY
09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
KMATERIALS FOR APPLICATIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
8Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
50Compositions for plastering borehole walls, i.e. compositions for temporary consolidation of borehole walls
504Compositions based on water or polar solvents
506containing organic compounds
508macromolecular compounds
514of natural origin, e.g. polysaccharides, cellulose
C09K 8/516 2006.1
CCHEMISTRY; METALLURGY
09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
KMATERIALS FOR APPLICATIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
8Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
50Compositions for plastering borehole walls, i.e. compositions for temporary consolidation of borehole walls
516characterised by their form or by the form of their components, e.g. encapsulated material
C08J 3/12 2006.1
CCHEMISTRY; METALLURGY
08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H142
3Processes of treating or compounding macromolecular substances
12Powdering or granulating
CPC
C08B 31/00
CCHEMISTRY; METALLURGY
08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
BPOLYSACCHARIDES; DERIVATIVES THEREOF
31Preparation of derivatives of starch
C08B 31/003
CCHEMISTRY; METALLURGY
08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
BPOLYSACCHARIDES; DERIVATIVES THEREOF
31Preparation of derivatives of starch
003Crosslinking of starch
C08B 31/12
CCHEMISTRY; METALLURGY
08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
BPOLYSACCHARIDES; DERIVATIVES THEREOF
31Preparation of derivatives of starch
08Ethers
12having alkyl or cycloalkyl radicals substituted by heteroatoms, ; e.g. hydroxyalkyl or carboxyalkyl starch
C08F 251/00
CCHEMISTRY; METALLURGY
08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
251Macromolecular compounds obtained by polymerising monomers on to polysaccharides or derivatives thereof
C08J 3/12
CCHEMISTRY; METALLURGY
08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G
3Processes of treating or compounding macromolecular substances
12Powdering or granulating
C09K 8/426
CCHEMISTRY; METALLURGY
09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
8Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
42Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells
426for plugging
Applicants
  • 中国石油化工股份有限公司 CHINA PETROLEUM & CHEMICAL CORPORATION [CN]/[CN]
  • 中国石油化工股份有限公司大连石油化工研究院 DALIAN RESEARCH INSTITUTE OF PETROLEUM AND PETROCHEMICALS, SINOPEC CORP. [CN]/[CN]
Inventors
  • 杨超 YANG, Chao
  • 王晨 WANG, Chen
  • 尹泽群 YIN, Zequn
  • 刘全杰 LIU, Quanjie
Agents
  • 北京润平知识产权代理有限公司 RUNPING & PARTNERS
Priority Data
201710720844.722.08.2017CN
201710720850.222.08.2017CN
201710720851.722.08.2017CN
201710720862.522.08.2017CN
201710720863.X22.08.2017CN
201710720864.422.08.2017CN
Publication Language Chinese (zh)
Filing Language Chinese (ZH)
Designated States
Title
(EN) STARCH-CONTAINING MICROSPHERE AND PREPARATION METHOD THEREFOR AND APPLICATION THEREOF
(FR) MICROSPHÈRE CONTENANT DE L'AMIDON ET PROCÉDÉ DE PRÉPARATION S'Y RAPPORTANT ET SON APPLICATION
(ZH) 一种含淀粉微球及其制备方法和应用
Abstract
(EN) Disclosed is a starch-containing microsphere and a preparation method therefor and an application thereof. The particle size of the starch-containing microsphere exhibits polydispersity with uniform distribution in a particle size concentrated distribution interval, and the particle size distribution in the particle size concentrated distribution interval has the following features: equal division of the particle size concentrated distribution interval into n intervals, and a microsphere percentage in each interval is (I), where n is an integer greater than 1. The preparation method comprises: first reacting starch with a low concentration of epichlorohydrin, and then reacting the resultant product with a surfactant, followed by final crosslinking to give microspheres. The starch-containing microspheres prepared by the present invention are polydisperse starch-containing microspheres with a uniform particle size distribution, with the particle size being in a range of 0.1-500 μm.
(FR) L'invention concerne une microsphère contenant de l'amidon, un procédé de préparation s'y rapportant et une application de celle-ci. La taille de particule de la microsphère contenant de l'amidon présente une polydispersité avec une distribution uniforme sur un étroit intervalle de distribution de la taille de particule et la distribution de la taille de particule dans l'étroit intervalle de distribution de la taille de particule a les caractéristiques suivantes : une division égale de l'étroit intervalle de distribution de la taille de particule en n intervalles et un pourcentage de microsphères dans chaque intervalle de (I), n étant un nombre entier supérieur à 1. Le procédé de préparation comprend : d'abord la réaction d'amidon avec une faible concentration d'épichlorhydrine, puis la réaction du produit ainsi obtenu avec un tensioactif, suivie d'une réticulation finale pour donner des microsphères. Les microsphères contenant de l'amidon préparées par la présente invention sont des microsphères contenant de l'amidon polydispersées ayant une distribution uniforme de la taille des particules, la taille des particules étant dans une plage de 0,1 à 500 µm.
(ZH) 公开了一种含淀粉微球及其制备方法和应用,所述含淀粉微球粒径在粒径集中分布区间内呈均匀分布的多分散性,所述粒径集中分布区间内的粒径分布具有如下特征:将粒径集中分布区间均分成n个区间,每个区间的微球占比为:(I) 其中n为大于1的整数。所述制备方法为,首先将淀粉与低浓度环氧氯丙烷反应,然后与表面活性剂作用,最后再进行交联得到微球。本发明制备的含淀粉微球是粒径均匀分布的多分散含淀粉微球,粒径为0.1~500μm。
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