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1. (WO2019027678) ACTIVATION OF NOBLE METAL CATALYSTS ON SILICEOUS SUPPORTS WITH WATER-CONTAINING GAS STREAM
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Pub. No.: WO/2019/027678 International Application No.: PCT/US2018/042692
Publication Date: 07.02.2019 International Filing Date: 18.07.2018
IPC:
B01J 38/06 (2006.01) ,B01J 38/02 (2006.01) ,B01J 29/04 (2006.01) ,B01J 29/068 (2006.01) ,B01J 29/74 (2006.01) ,B01J 35/00 (2006.01) ,B01J 37/10 (2006.01) ,B01J 37/18 (2006.01) ,B01J 37/00 (2006.01) ,B01J 29/90 (2006.01) ,B01J 38/10 (2006.01) ,C10G 45/00 (2006.01) ,B01J 8/04 (2006.01) ,B01J 8/02 (2006.01)
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
38
Regeneration or reactivation of catalysts, in general
04
Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
06
using steam
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
38
Regeneration or reactivation of catalysts, in general
02
Heat treatment
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
29
Catalysts comprising molecular sieves
04
having base-exchange properties, e.g. crystalline zeolites, pillared clays
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
29
Catalysts comprising molecular sieves
04
having base-exchange properties, e.g. crystalline zeolites, pillared clays
06
Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
064
containing iron group metals, noble metals or copper
068
Noble metals
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
29
Catalysts comprising molecular sieves
04
having base-exchange properties, e.g. crystalline zeolites, pillared clays
06
Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
70
of types characterised by their specific structure not provided for in groups B01J29/08-B01J29/65130
72
containing iron group metals, noble metals or copper
74
Noble metals
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
35
Catalysts, in general, characterised by their form or physical properties
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
37
Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
08
Heat treatment
10
in the presence of water, e.g. steam
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
37
Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
16
Reducing
18
with gases containing free hydrogen
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
37
Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
29
Catalysts comprising molecular sieves
90
Regeneration or reactivation
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
38
Regeneration or reactivation of catalysts, in general
04
Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
10
using elemental hydrogen
C CHEMISTRY; METALLURGY
10
PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
G
CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
45
Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
8
Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
02
with stationary particles, e.g. in fixed beds
04
the fluid passing successively through two or more beds
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
8
Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
02
with stationary particles, e.g. in fixed beds
Applicants:
EXXONMOBIL RESEARCH AND ENGINEERING COMPANY [US/US]; 1545 Route 22 East P.O. Box 900 Annandale, NJ 08801-0900, US
Inventors:
McCARTHY, Stephen, J.; US
PODSIADLO, Paul; US
SCHLEICHER, Gary, P.; US
HILBERT, Timothy, L.; US
HOO, Teck-mui; US
JOSECK, Eric, D.; US
Agent:
WRKICH, Joseph, E.; US
NEGRON, Liza; US
BARRETT, Glenn, T.; US
YARNELL, Scott, F.; US
MIGLIORINI, Robert, A.; US
Priority Data:
62/540,65403.08.2017US
Title (EN) ACTIVATION OF NOBLE METAL CATALYSTS ON SILICEOUS SUPPORTS WITH WATER-CONTAINING GAS STREAM
(FR) ACTIVATION DE CATALYSEURS DE MÉTAUX NOBLES SUR DES SUPPORTS SILICEUX AVEC UN FLUX DE GAZ CONTENANT DE L'EAU
Abstract:
(EN) Systems and methods are provided for activation of noble metal catalysts that are supported on siliceous supports. The activation method can include limiting the amount of water vapor pressure and/or the time of exposure to the water vapor pressure during heating of the catalyst at temperatures of 50°C or less. This can be achieved by introducing heated gas into multiple reactors of a multi-reactor system at the same time. A suitable system for introducing heated gas into multiple reactors can correspond to a system with multiple heated hydrogen lines for delivery of heated hydrogen to a plurality of reactors within a multi-reactor system.
(FR) L'invention concerne des systèmes et des procédés pour l'activation de catalyseurs de métaux nobles qui sont supportés sur des supports siliceux. Le procédé d'activation peut comprendre la limitation de la quantité de pression de vapeur d'eau et/ou du temps d'exposition à la pression de vapeur d'eau pendant le chauffage du catalyseur à des températures de 50 °C ou moins. Ceci peut être obtenu par introduction d'un gaz chauffé dans de multiples réacteurs d'un système multi-réacteurs en même temps. Un système approprié pour introduire un gaz chauffé dans de multiples réacteurs peut correspondre à un système ayant de multiples conduites d'hydrogène chauffées pour l'administration d'hydrogène chauffé à une pluralité de réacteurs dans un système multi-réacteurs.
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Designated States: AE, AG, AL, AM, AO, AT, AU, AZ, BA, BB, BG, BH, BN, BR, BW, BY, BZ, CA, CH, CL, CN, CO, CR, CU, CZ, DE, DJ, DK, DM, DO, DZ, EC, EE, EG, ES, FI, GB, GD, GE, GH, GM, GT, HN, HR, HU, ID, IL, IN, IR, IS, JO, JP, KE, KG, KH, KN, KP, KR, KW, KZ, LA, LC, LK, LR, LS, LU, LY, MA, MD, ME, MG, MK, MN, MW, MX, MY, MZ, NA, NG, NI, NO, NZ, OM, PA, PE, PG, PH, PL, PT, QA, RO, RS, RU, RW, SA, SC, SD, SE, SG, SK, SL, SM, ST, SV, SY, TH, TJ, TM, TN, TR, TT, TZ, UA, UG, US, UZ, VC, VN, ZA, ZM, ZW
African Regional Intellectual Property Organization (ARIPO) (BW, GH, GM, KE, LR, LS, MW, MZ, NA, RW, SD, SL, ST, SZ, TZ, UG, ZM, ZW)
Eurasian Patent Office (AM, AZ, BY, KG, KZ, RU, TJ, TM)
European Patent Office (EPO) (AL, AT, BE, BG, CH, CY, CZ, DE, DK, EE, ES, FI, FR, GB, GR, HR, HU, IE, IS, IT, LT, LU, LV, MC, MK, MT, NL, NO, PL, PT, RO, RS, SE, SI, SK, SM, TR)
African Intellectual Property Organization (BF, BJ, CF, CG, CI, CM, GA, GN, GQ, GW, KM, ML, MR, NE, SN, TD, TG)
Publication Language: English (EN)
Filing Language: English (EN)