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1. (WO2018225834) EPOXY-AMINE ADDUCT, THERMOPLASTIC RESIN COMPOSITION, SIZING AGENT, SIZING AGENT-COATED CARBON FIBERS, AND FIBER-REINFORCED COMPOSITE MATERIAL
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Pub. No.: WO/2018/225834 International Application No.: PCT/JP2018/021929
Publication Date: 13.12.2018 International Filing Date: 07.06.2018
IPC:
C08G 59/24 (2006.01) ,C08G 59/50 (2006.01) ,C08J 5/24 (2006.01) ,C08L 75/00 (2006.01) ,C08L 101/00 (2006.01) ,C09D 5/02 (2006.01) ,C09D 163/00 (2006.01) ,D06M 15/55 (2006.01) ,D06M 15/564 (2006.01) ,D06M 101/40 (2006.01)
C CHEMISTRY; METALLURGY
08
ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
G
MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
59
Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by reaction of epoxy polycondensates with monofunctional low-molecular-weight compounds; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
18
Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
20
characterised by the epoxy compounds used
22
Di-epoxy compounds
24
carbocyclic
C CHEMISTRY; METALLURGY
08
ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
G
MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
59
Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by reaction of epoxy polycondensates with monofunctional low-molecular-weight compounds; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
18
Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
40
characterised by the curing agents used
50
Amines
C CHEMISTRY; METALLURGY
08
ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
J
WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H142
5
Manufacture of articles or shaped materials containing macromolecular substances
24
Impregnating materials with prepolymers which can be polymerised in situ, e.g. manufacture of prepregs
C CHEMISTRY; METALLURGY
08
ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
L
COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
75
Compositions of polyureas or polyurethanes; Compositions of derivatives of such polymers
C CHEMISTRY; METALLURGY
08
ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
L
COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
101
Compositions of unspecified macromolecular compounds
C CHEMISTRY; METALLURGY
09
DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
D
COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
5
Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
02
Emulsion paints
C CHEMISTRY; METALLURGY
09
DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
D
COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
163
Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
D TEXTILES; PAPER
06
TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
M
TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D0664
15
Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials with macromolecular compounds; Such treatment combined with mechanical treatment
19
with synthetic macromolecular compounds
37
Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
55
Epoxy resins
D TEXTILES; PAPER
06
TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
M
TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D0664
15
Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials with macromolecular compounds; Such treatment combined with mechanical treatment
19
with synthetic macromolecular compounds
37
Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
564
Polyureas, polyurethanes or other polymers having ureide or urethane links; Precondensation products forming them
D TEXTILES; PAPER
06
TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
M
TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D0664
101
Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
40
Fibres of carbon
Applicants:
株式会社ダイセル DAICEL CORPORATION [JP/JP]; 大阪府大阪市北区大深町3番1号 3-1, Ofuka-cho, Kita-ku, Osaka-shi, Osaka 5300011, JP
Inventors:
井上寛子 INOUE, Hiroko; JP
Agent:
特許業務法人後藤特許事務所 GOTO & CO.; 大阪府大阪市北区紅梅町2番18号 2-18, Kobai-cho, Kita-ku, Osaka-shi, Osaka 5300038, JP
Priority Data:
2017-11303607.06.2017JP
Title (EN) EPOXY-AMINE ADDUCT, THERMOPLASTIC RESIN COMPOSITION, SIZING AGENT, SIZING AGENT-COATED CARBON FIBERS, AND FIBER-REINFORCED COMPOSITE MATERIAL
(FR) ADDUIT ÉPOXY-AMINE, COMPOSITION DE RÉSINE THERMOPLASTIQUE, AGENT D'ENCOLLAGE, FIBRE DE CARBONE REVÊTUE DE PRODUIT D'ENCOLLAGE ET MATÉRIAU COMPOSITE RENFORCÉ DE FIBRES
(JA) エポキシ-アミン付加物、熱可塑性樹脂組成物、サイジング剤、サイジング剤塗布炭素繊維、及び繊維強化複合材料
Abstract:
(EN) The purpose of the present invention is to provide a compound which is capable of forming a polymer composite (such as a fiber-reinforced composite material) having excellent mechanical properties (especially, toughness), while being easily blended with other components such as resins, and which is also capable of improving adhesion between a resin and an additive in the polymer composite. The present invention provides an epoxy-amine adduct which is a compound [I] having two or more amino groups in each molecule or a salt thereof, and which has amino groups at both ends. The compound [I] is an adduct of an epoxy compound (A) that has two or more alicyclic epoxy groups in each molecule and an amine compound (B) that has two or more amino groups in each molecule; the epoxy compound (A) contains a compound of formula (a); and the amine compound (B) contains at least one compound selected from among compounds of formula (b-I) and at least one compound selected from among compounds of formula (b-II). (In the formulae, the symbols are as defined in the description.)
(FR) La présente invention vise à fournir un composé qui est capable de former un composite polymère (tel qu'un matériau composite renforcé par des fibres) ayant d'excellentes propriétés mécaniques (en particulier, la ténacité), tout en étant facilement mélangé avec d'autres composants tels que des résines, et qui est également capable d'améliorer l'adhérence entre une résine et un additif dans le composite polymère. La présente invention concerne un adduit époxy-amine qui est un composé [I] ayant deux groupes amino ou plus dans chaque molécule ou un sel de celui-ci, et qui a des groupes amino au niveau des deux extrémités. Le composé [I] est un adduit d'un composé époxy (A) qui a deux groupes époxy alicycliques ou plus dans chaque molécule et un composé amine (B) qui a deux groupes amino ou plus dans chaque molécule ; le composé époxy (A) contient un composé de formule (a) ; et le composé amine (B) contient au moins un composé sélectionné parmi les composés de formule (b-I) et au moins un composé sélectionné parmi les composés de formule (b-II). (Dans les formules, les symboles sont tels que définis dans la description.)
(JA) 本発明は、ポリマー系コンポジットにおける樹脂と添加材との密着性を向上させることができ、樹脂等の他の成分に対する配合が容易であると共に、機械物性(特に、強靭性)に優れるポリマー系コンポジット(繊維強化複合材料等)を形成できる化合物を提供することを目的とする。 本発明は、分子内に2個以上のアミノ基を有する化合物[I]、又はその塩であって、 化合物[I]が、分子内に2個以上の脂環式エポキシ基を有するエポキシ化合物(A)と、分子内に2個以上のアミノ基を有するアミン化合物(B)との付加物であり、 エポキシ化合物(A)が、下記式(a)の化合物を含み、 アミン化合物(B)が、下記式(b-I)の化合物から選ばれる少なくとも1種、及び下記式(b-II)の化合物から選ばれる少なくとも1種を含み、 両末端にアミノ基を有する化合物であるエポキシ-アミン付加物を提供する。 [式中、各記号は、明細書で定義される通りである。]
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Designated States: AE, AG, AL, AM, AO, AT, AU, AZ, BA, BB, BG, BH, BN, BR, BW, BY, BZ, CA, CH, CL, CN, CO, CR, CU, CZ, DE, DJ, DK, DM, DO, DZ, EC, EE, EG, ES, FI, GB, GD, GE, GH, GM, GT, HN, HR, HU, ID, IL, IN, IR, IS, JO, JP, KE, KG, KH, KN, KP, KR, KW, KZ, LA, LC, LK, LR, LS, LU, LY, MA, MD, ME, MG, MK, MN, MW, MX, MY, MZ, NA, NG, NI, NO, NZ, OM, PA, PE, PG, PH, PL, PT, QA, RO, RS, RU, RW, SA, SC, SD, SE, SG, SK, SL, SM, ST, SV, SY, TH, TJ, TM, TN, TR, TT, TZ, UA, UG, US, UZ, VC, VN, ZA, ZM, ZW
African Regional Intellectual Property Organization (ARIPO) (BW, GH, GM, KE, LR, LS, MW, MZ, NA, RW, SD, SL, ST, SZ, TZ, UG, ZM, ZW)
Eurasian Patent Office (AM, AZ, BY, KG, KZ, RU, TJ, TM)
European Patent Office (EPO) (AL, AT, BE, BG, CH, CY, CZ, DE, DK, EE, ES, FI, FR, GB, GR, HR, HU, IE, IS, IT, LT, LU, LV, MC, MK, MT, NL, NO, PL, PT, RO, RS, SE, SI, SK, SM, TR)
African Intellectual Property Organization (BF, BJ, CF, CG, CI, CM, GA, GN, GQ, GW, KM, ML, MR, NE, SN, TD, TG)
Publication Language: Japanese (JA)
Filing Language: Japanese (JA)