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1. (WO2018162363) SERIAL PROCESS FOR CONVERTING SYNGAS TO LIQUID HYDROCARBONS, DEVICE USED THEREFOR INCLUDING FT- AND HT-CATALYSTS, FT-CATALYST
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Pub. No.: WO/2018/162363 International Application No.: PCT/EP2018/055237
Publication Date: 13.09.2018 International Filing Date: 04.03.2018
IPC:
B01J 23/46 (2006.01) ,B01J 23/745 (2006.01) ,B01J 23/75 (2006.01) ,B01J 23/89 (2006.01) ,B01J 29/04 (2006.01) ,B01J 29/44 (2006.01) ,B01J 35/02 (2006.01) ,B01J 35/10 (2006.01) ,B01J 37/08 (2006.01) ,B01J 37/02 (2006.01) ,B01J 37/00 (2006.01) ,C07C 1/04 (2006.01) ,C10G 2/00 (2006.01) ,C07C 5/22 (2006.01) ,C07C 5/27 (2006.01) ,B01J 35/00 (2006.01) ,B01J 37/18 (2006.01)
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
23
Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/113
38
of noble metals
40
of the platinum group metals
46
Ruthenium, rhodium, osmium or iridium
B PERFORMING OPERATIONS; TRANSPORTING
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PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
23
Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/113
70
of the iron group metals or copper
74
Iron group metals
745
Iron
B PERFORMING OPERATIONS; TRANSPORTING
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PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
23
Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/113
70
of the iron group metals or copper
74
Iron group metals
75
Cobalt
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
23
Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/113
70
of the iron group metals or copper
89
combined with noble metals
B PERFORMING OPERATIONS; TRANSPORTING
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PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
29
Catalysts comprising molecular sieves
04
having base-exchange properties, e.g. crystalline zeolites, pillared clays
B PERFORMING OPERATIONS; TRANSPORTING
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PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
29
Catalysts comprising molecular sieves
04
having base-exchange properties, e.g. crystalline zeolites, pillared clays
06
Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
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of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11
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containing iron group metals, noble metals or copper
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Noble metals
B PERFORMING OPERATIONS; TRANSPORTING
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PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
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Catalysts, in general, characterised by their form or physical properties
02
Solids
B PERFORMING OPERATIONS; TRANSPORTING
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PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
35
Catalysts, in general, characterised by their form or physical properties
02
Solids
10
characterised by their surface properties or porosity
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
37
Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
08
Heat treatment
B PERFORMING OPERATIONS; TRANSPORTING
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PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
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Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
02
Impregnation, coating or precipitation
B PERFORMING OPERATIONS; TRANSPORTING
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PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
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Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
C CHEMISTRY; METALLURGY
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ORGANIC CHEMISTRY
C
ACYCLIC OR CARBOCYCLIC COMPOUNDS
1
Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon
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from oxides of carbon
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from carbon monoxide with hydrogen
C CHEMISTRY; METALLURGY
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PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
G
CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
2
Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon
C CHEMISTRY; METALLURGY
07
ORGANIC CHEMISTRY
C
ACYCLIC OR CARBOCYCLIC COMPOUNDS
5
Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms
22
by isomerisation
C CHEMISTRY; METALLURGY
07
ORGANIC CHEMISTRY
C
ACYCLIC OR CARBOCYCLIC COMPOUNDS
5
Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms
22
by isomerisation
27
Rearrangement of carbon atoms in the hydrocarbon skeleton
B PERFORMING OPERATIONS; TRANSPORTING
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PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
35
Catalysts, in general, characterised by their form or physical properties
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
37
Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
16
Reducing
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with gases containing free hydrogen
Applicants:
STUDIENGESELLSCHAFT KOHLE MBH [DE/DE]; Kaiser-Wilhelm-Platz 1 45470 Mülheim, DE
Inventors:
SCHÜTH, Ferdi; DE
PRIETO-GONZALEZ, Gonzalo; DE
DUYCKAERTS, Nicolas; DE
Priority Data:
10 2017 104 605.406.03.2017DE
Title (EN) SERIAL PROCESS FOR CONVERTING SYNGAS TO LIQUID HYDROCARBONS, DEVICE USED THEREFOR INCLUDING FT- AND HT-CATALYSTS, FT-CATALYST
(FR) PROCÉDÉ SÉRIE DE CONVERSION DE GAZ DE SYNTHÈSE EN HYDROCARBURES LIQUIDES, DISPOSITIF UTILISÉ À CET EFFET COMPRENANT DES CATALYSEURS FT ET HT, CATALYSEUR FT
Abstract:
(EN) The invention relates, in a first aspect, to a process to convert a feed stream comprising carbon monoxide and hydrogen as major components (synthesis gas) into liquid hydrocarbons by means of the combination of a Fischer-Tropsch solid catalyst and a hydrotreating solid catalyst in separate catalyst beds operated at different reaction temperatures, and, in a second aspect, to a multimodal porosity Fischer-Tropsch catalyst to be applied in said process and the method for preparing said Fischer-Tropsch catalyst.
(FR) Selon un premier aspect, l'invention concerne un procédé de conversion d'un débit d'entrée comprenant du monoxyde de carbone et de l'hydrogène en tant que composants majeurs (gaz de synthèse) en hydrocarbures liquides au moyen de la combinaison d'un catalyseur solide de Fischer-Tropsch et d'un catalyseur solide d'hydrotraitement dans des lits de catalyseur séparés fonctionnant à différentes températures de réaction. Dans un second aspect, l'invention concerne un catalyseur de Fischer-Tropsch à porosité multimodale à appliquer dans ledit procédé et le procédé de préparation dudit catalyseur de Fischer-Tropsch.
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Designated States: AE, AG, AL, AM, AO, AT, AU, AZ, BA, BB, BG, BH, BN, BR, BW, BY, BZ, CA, CH, CL, CN, CO, CR, CU, CZ, DE, DJ, DK, DM, DO, DZ, EC, EE, EG, ES, FI, GB, GD, GE, GH, GM, GT, HN, HR, HU, ID, IL, IN, IR, IS, JO, JP, KE, KG, KH, KN, KP, KR, KW, KZ, LA, LC, LK, LR, LS, LU, LY, MA, MD, ME, MG, MK, MN, MW, MX, MY, MZ, NA, NG, NI, NO, NZ, OM, PA, PE, PG, PH, PL, PT, QA, RO, RS, RU, RW, SA, SC, SD, SE, SG, SK, SL, SM, ST, SV, SY, TH, TJ, TM, TN, TR, TT, TZ, UA, UG, US, UZ, VC, VN, ZA, ZM, ZW
African Regional Intellectual Property Organization (ARIPO) (BW, GH, GM, KE, LR, LS, MW, MZ, NA, RW, SD, SL, ST, SZ, TZ, UG, ZM, ZW)
Eurasian Patent Office (AM, AZ, BY, KG, KZ, RU, TJ, TM)
European Patent Office (EPO) (AL, AT, BE, BG, CH, CY, CZ, DE, DK, EE, ES, FI, FR, GB, GR, HR, HU, IE, IS, IT, LT, LU, LV, MC, MK, MT, NL, NO, PL, PT, RO, RS, SE, SI, SK, SM, TR)
African Intellectual Property Organization (BF, BJ, CF, CG, CI, CM, GA, GN, GQ, GW, KM, ML, MR, NE, SN, TD, TG)
Publication Language: English (EN)
Filing Language: English (EN)