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1. (WO2018159595) CATALYST FOR HYDROSILYLATION REACTION, HYDROGENATION REACTION, AND HYDROSILANE REDUCTION REACTION
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Pub. No.: WO/2018/159595 International Application No.: PCT/JP2018/007204
Publication Date: 07.09.2018 International Filing Date: 27.02.2018
IPC:
B01J 31/22 (2006.01) ,C07C 5/03 (2006.01) ,C07C 9/15 (2006.01) ,C07C 15/073 (2006.01) ,C07C 209/50 (2006.01) ,C07C 211/27 (2006.01) ,C07F 7/08 (2006.01) ,C07F 7/10 (2006.01) ,C08G 77/08 (2006.01) ,C07B 61/00 (2006.01)
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
31
Catalysts comprising hydrides, coordination complexes or organic compounds
16
containing coordination complexes
22
Organic complexes
C CHEMISTRY; METALLURGY
07
ORGANIC CHEMISTRY
C
ACYCLIC OR CARBOCYCLIC COMPOUNDS
5
Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms
02
by hydrogenation
03
of non-aromatic carbon-to-carbon double bonds
C CHEMISTRY; METALLURGY
07
ORGANIC CHEMISTRY
C
ACYCLIC OR CARBOCYCLIC COMPOUNDS
9
Acyclic saturated hydrocarbons
14
with five to fifteen carbon atoms
15
Straight-chain hydrocarbons
C CHEMISTRY; METALLURGY
07
ORGANIC CHEMISTRY
C
ACYCLIC OR CARBOCYCLIC COMPOUNDS
15
Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic part
02
Monocyclic hydrocarbons
067
C8H10 hydrocarbons
073
Ethylbenzene
C CHEMISTRY; METALLURGY
07
ORGANIC CHEMISTRY
C
ACYCLIC OR CARBOCYCLIC COMPOUNDS
209
Preparation of compounds containing amino groups bound to a carbon skeleton
44
by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
50
by reduction of carboxylic acid amides
C CHEMISTRY; METALLURGY
07
ORGANIC CHEMISTRY
C
ACYCLIC OR CARBOCYCLIC COMPOUNDS
211
Compounds containing amino groups bound to a carbon skeleton
01
having amino groups bound to acyclic carbon atoms
26
of an unsaturated carbon skeleton containing at least one six-membered aromatic ring
27
having amino groups linked to the six-membered aromatic ring by saturated carbon chains
C CHEMISTRY; METALLURGY
07
ORGANIC CHEMISTRY
F
ACYCLIC, CARBOCYCLIC, OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
7
Compounds containing elements of the 4th Group of the Periodic System
02
Silicon compounds
08
Compounds having one or more C-Si linkages
C CHEMISTRY; METALLURGY
07
ORGANIC CHEMISTRY
F
ACYCLIC, CARBOCYCLIC, OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
7
Compounds containing elements of the 4th Group of the Periodic System
02
Silicon compounds
08
Compounds having one or more C-Si linkages
10
containing nitrogen
C CHEMISTRY; METALLURGY
08
ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
G
MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
77
Macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon
04
Polysiloxanes
06
Preparatory processes
08
characterised by the catalysts used
C CHEMISTRY; METALLURGY
07
ORGANIC CHEMISTRY
B
GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
61
Other general methods
Applicants:
国立大学法人九州大学 KYUSHU UNIVERSITY, NATIONAL UNIVERSITY CORPORATION [JP/JP]; 福岡県福岡市東区箱崎六丁目10番1号 6-10-1, Hakozaki, Higashi-ku, Fukuoka-shi, Fukuoka 8128581, JP
信越化学工業株式会社 SHIN-ETSU CHEMICAL CO., LTD. [JP/JP]; 東京都千代田区大手町二丁目6番1号 6-1, Ohtemachi 2-chome, Chiyoda-ku, Tokyo 1000004, JP
Inventors:
永島 英夫 NAGASHIMA Hideo; JP
真川 敦嗣 SANAGAWA Atsushi; JP
川端 将真 KAWABATA Shoma; JP
野田 大輔 NODA Daisuke; JP
作田 晃司 SAKUTA Koji; JP
Agent:
特許業務法人英明国際特許事務所 PATENT PROFESSIONAL CORPORATION EI-MEI PATENT OFFICE; 東京都中央区銀座二丁目16番12号 銀座大塚ビル2階 GINZA OHTSUKA Bldg. 2F, 16-12, Ginza 2-chome, Chuo-ku, Tokyo 1040061, JP
Priority Data:
2017-03694628.02.2017JP
Title (EN) CATALYST FOR HYDROSILYLATION REACTION, HYDROGENATION REACTION, AND HYDROSILANE REDUCTION REACTION
(FR) CATALYSEUR POUR RÉACTION D’HYDROSILYLATION, RÉACTION D’HYDROGÉNATION, ET RÉACTION DE RÉDUCTION PAR HYDROSILANE
(JA) ヒドロシリル化反応、水素化反応およびヒドロシラン還元反応用触媒
Abstract:
(EN) Provided is a catalyst which comprises a compound represented by formula (1) and which exhibits activity for at least one type of reaction selected from among hydrosilylation reaction or hydrogenation reaction with respect to an aliphatic unsaturated bond and hydrosilane reduction reaction with respect to a carbon-oxygen unsaturated bond or a carbon-nitrogen unsaturated bond. Formula (1): Mn(Lm) {M represents Fe, Co, or Ni having an oxidation number of 0, L represents an isocyanide ligand represented by formula (2), n denotes an integer of 1-8, and m denotes an integer of 2-12. Formula (2): (CN)x-R1 (R1 represents a mono- to trivalent-organic group having 1-30 carbon atoms, optionally being substituted by a halogen atom, and optionally having interposed therein one or more atoms selected from among O, N, S, and Si; and x denotes an integer of 1-3.)}.
(FR) L’invention concerne un catalyseur qui est constitué d’un composé de formule (1), et qui est actif dans au moins une sorte de réaction choisie parmi soit une réaction d’hydrosilylation ou une réaction d’hydrogénation vis-à-vis d’une liaison insaturée aliphatique, soit une réaction de réduction par hydrosilane vis-à-vis d’une liaison insaturée carbone-oxygène ou d’une liaison insaturée carbone-azote. Mn(L)m (1) {M représente un Fe, Co ou Ni d’état d’oxydation de valence 0, L représente un ligand isocynure représenté par la formule (2), n représente un nombre entier de 1 à 8, et m représente un nombre entier de 2 à 12. (CN)x-R1 (2) (R1 représente un groupe organique de valence comprise entre 1 et 3 et de nombre d’atomes de carbone compris entre 1 et 30 qui peut être substitué par un atome d’halogène, et dans lequel un atome ou plus choisi parmi O, N , S et Si peut s’intercaler.)}
(JA) 式(1)の化合物からなり、脂肪族不飽和結合に対するヒドロシリル化反応もしくは水素化反応、または炭素-酸素不飽和結合もしくは炭素-窒素不飽和結合に対するヒドロシラン還元反応から選ばれる少なくとも1種の反応に活性を有する触媒。 Mn(L)m (1) {Mは酸化数が0価のFe、Co、またはNiを、Lは下記式(2)で示されるイソシアニド配位子を、nは1~8の整数を、mは2~12の整数を表す。 (CN)x-R1 (2) (R1はハロゲン原子で置換されていてもよく、O、N、SおよびSiから選ばれる原子が1個以上介在してもよい、炭素原子数1~30の1~3価の有機基を、xは1~3の整数を表す。)}
Designated States: AE, AG, AL, AM, AO, AT, AU, AZ, BA, BB, BG, BH, BN, BR, BW, BY, BZ, CA, CH, CL, CN, CO, CR, CU, CZ, DE, DJ, DK, DM, DO, DZ, EC, EE, EG, ES, FI, GB, GD, GE, GH, GM, GT, HN, HR, HU, ID, IL, IN, IR, IS, JO, JP, KE, KG, KH, KN, KP, KR, KW, KZ, LA, LC, LK, LR, LS, LU, LY, MA, MD, ME, MG, MK, MN, MW, MX, MY, MZ, NA, NG, NI, NO, NZ, OM, PA, PE, PG, PH, PL, PT, QA, RO, RS, RU, RW, SA, SC, SD, SE, SG, SK, SL, SM, ST, SV, SY, TH, TJ, TM, TN, TR, TT, TZ, UA, UG, US, UZ, VC, VN, ZA, ZM, ZW
African Regional Intellectual Property Organization (ARIPO) (BW, GH, GM, KE, LR, LS, MW, MZ, NA, RW, SD, SL, ST, SZ, TZ, UG, ZM, ZW)
Eurasian Patent Office (AM, AZ, BY, KG, KZ, RU, TJ, TM)
European Patent Office (EPO) (AL, AT, BE, BG, CH, CY, CZ, DE, DK, EE, ES, FI, FR, GB, GR, HR, HU, IE, IS, IT, LT, LU, LV, MC, MK, MT, NL, NO, PL, PT, RO, RS, SE, SI, SK, SM, TR)
African Intellectual Property Organization (BF, BJ, CF, CG, CI, CM, GA, GN, GQ, GW, KM, ML, MR, NE, SN, TD, TG)
Publication Language: Japanese (JA)
Filing Language: Japanese (JA)