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1. (WO2018039105) A POLAR ADDITIVE-CONTAINING HYDROPROCESSING CATALYST, ITS PREPARATION AND USE
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Pub. No.: WO/2018/039105 International Application No.: PCT/US2017/047739
Publication Date: 01.03.2018 International Filing Date: 21.08.2017
IPC:
B01J 37/18 (2006.01) ,B01J 37/20 (2006.01) ,B01J 23/75 (2006.01) ,B01J 23/755 (2006.01) ,B01J 23/882 (2006.01) ,B01J 23/883 (2006.01) ,B01J 23/888 (2006.01) ,B01J 27/185 (2006.01) ,B01J 31/02 (2006.01) ,B01J 31/04 (2006.01) ,B01J 37/02 (2006.01) ,C10G 45/08 (2006.01) ,B01J 37/08 (2006.01)
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
37
Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
16
Reducing
18
with gases containing free hydrogen
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
37
Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
20
Sulfiding
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
23
Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/113
70
of the iron group metals or copper
74
Iron group metals
75
Cobalt
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
23
Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/113
70
of the iron group metals or copper
74
Iron group metals
755
Nickel
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
23
Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/113
70
of the iron group metals or copper
76
combined with metals, oxides or hydroxides provided for in groups B01J23/02-B01J23/36118
84
with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
85
Chromium, molybdenum, or tungsten
88
Molybdenum
882
and cobalt
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
23
Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/113
70
of the iron group metals or copper
76
combined with metals, oxides or hydroxides provided for in groups B01J23/02-B01J23/36118
84
with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
85
Chromium, molybdenum, or tungsten
88
Molybdenum
883
and nickel
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
23
Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/113
70
of the iron group metals or copper
76
combined with metals, oxides or hydroxides provided for in groups B01J23/02-B01J23/36118
84
with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
85
Chromium, molybdenum, or tungsten
888
Tungsten
B PERFORMING OPERATIONS; TRANSPORTING
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PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
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Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
14
Phosphorus; Compounds thereof
185
with iron group metals or platinum group metals
B PERFORMING OPERATIONS; TRANSPORTING
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PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
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Catalysts comprising hydrides, coordination complexes or organic compounds
02
containing organic compounds or metal hydrides
B PERFORMING OPERATIONS; TRANSPORTING
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PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
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Catalysts comprising hydrides, coordination complexes or organic compounds
02
containing organic compounds or metal hydrides
04
containing carboxylic acids or their salts
B PERFORMING OPERATIONS; TRANSPORTING
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PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
37
Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
02
Impregnation, coating or precipitation
C CHEMISTRY; METALLURGY
10
PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
G
CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
45
Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
02
to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing
04
characterised by the catalyst used
06
containing nickel or cobalt metal, or compounds thereof
08
in combination with chromium, molybdenum, or tungsten metals, or compounds thereof
B PERFORMING OPERATIONS; TRANSPORTING
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PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
37
Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
08
Heat treatment
Applicants: SHELL OIL COMPANY[US/US]; P.O. Box 576 Houston, Texas 77001-0576, US (US)
SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V.[NL/NL]; Carel van Bylandtlaan 30 NL-2596 The Hague, NL (AE, AG, AL, AM, AO, AT, AU, AZ, BA, BB, BE, BF, BG, BH, BJ, BN, BR, BW, BY, BZ, CA, CF, CG, CH, CI, CL, CM, CN, CO, CR, CU, CY, CZ, DE, DJ, DK, DM, DO, DZ, EC, EE, EG, ES, FI, FR, GA, GB, GD, GE, GH, GM, GN, GQ, GR, GT, GW, HN, HR, HU, ID, IE, IL, IN, IR, IS, IT, JO, JP, KE, KG, KH, KM, KN, KP, KR, KW, KZ, LA, LC, LK, LR, LS, LT, LU, LV, LY, MA, MC, MD, ME, MG, MK, ML, MN, MR, MT, MW, MX, MY, MZ, NA, NE, NG, NI, NL, NO, NZ, OM, PA, PE, PG, PH, PL, PT, QA, RO, RS, RU, RW, SA, SC, SD, SE, SG, SI, SK, SL, SM, SN, ST, SV, SY, SZ, TD, TG, TH, TJ, TM, TN, TR, TT, TZ, UA, UG, UZ, VC, VN, ZA, ZM, ZW)
Inventors: KRUEGER, Karl Marvin; US
Agent: STEWART, Charles W.; US
Priority Data:
62/378,31123.08.2016US
Title (EN) A POLAR ADDITIVE-CONTAINING HYDROPROCESSING CATALYST, ITS PREPARATION AND USE
(FR) CATALYSEUR D'HYDROTRAITEMENT CONTENANT UN ADDITIF POLAIRE, SA PRÉPARATION ET SON UTILISATION
Abstract:
(EN) A catalyst composition, its use in hydroprocessing of hydrocarbons, preferably middle-distillates such as diesel, and a method of making it, comprising impregnating a support material, preferably gamma-alumina extrudates, with 0.5-20 wt.% Co,Ni and 5-50 wt.% Mo,W metals and a di- or tricarboxylic acid of specified MW and carbon atom content, preferably gluconic or citric acid, followed by a controlled drying of the impregnated support, the temperature being within the liquid range of the carboxylic acid used, and incorporation thereafter of a non-S containing heterocompound with D >= 0.45 as further additive, preferably selected from lactams, cyclic esters or cyclic ethers, in particular NMP or propylene carbonate, into the dried, impregnated support.
(FR) L'invention concerne une composition de catalyseur, son utilisation dans l'hydrotraitement d'hydrocarbures, de préférence des distillats moyens tels que le diesel, et son procédé de fabrication, comprenant l'imprégnation d'un matériau de support, de préférence des extrudés de gamma-alumine, avec 0,5 à 20 % en poids de Co,Ni, et 5 à 50 % en poidsde Mo,W et d'un acide di- ou tricarboxylique de poids moléculaire et d'atomes de carbone spécifiés, de préférence de l'acide gluconique ou citrique, suivi d'un séchage contrôlé du support imprégné, la température étant compris dans la plage liquide de l'acide carboxylique utilisé, et incorporation par la suite d'un hétérocomposé contenant du S avec D> = 0,45 en tant qu'additif supplémentaire, de préférence choisi parmi les lactames, des esters cycliques ou des éthers cycliques, en particulier NMP ou carbonate de propylène, dans le support imprégné séché.
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Designated States: AE, AG, AL, AM, AO, AT, AU, AZ, BA, BB, BG, BH, BN, BR, BW, BY, BZ, CA, CH, CL, CN, CO, CR, CU, CZ, DE, DJ, DK, DM, DO, DZ, EC, EE, EG, ES, FI, GB, GD, GE, GH, GM, GT, HN, HR, HU, ID, IL, IN, IR, IS, JO, JP, KE, KG, KH, KN, KP, KR, KW, KZ, LA, LC, LK, LR, LS, LU, LY, MA, MD, ME, MG, MK, MN, MW, MX, MY, MZ, NA, NG, NI, NO, NZ, OM, PA, PE, PG, PH, PL, PT, QA, RO, RS, RU, RW, SA, SC, SD, SE, SG, SK, SL, SM, ST, SV, SY, TH, TJ, TM, TN, TR, TT, TZ, UA, UG, US, UZ, VC, VN, ZA, ZM, ZW
African Regional Intellectual Property Organization (ARIPO) (BW, GH, GM, KE, LR, LS, MW, MZ, NA, RW, SD, SL, ST, SZ, TZ, UG, ZM, ZW)
Eurasian Patent Office (AM, AZ, BY, KG, KZ, RU, TJ, TM)
European Patent Office (EPO) (AL, AT, BE, BG, CH, CY, CZ, DE, DK, EE, ES, FI, FR, GB, GR, HR, HU, IE, IS, IT, LT, LU, LV, MC, MK, MT, NL, NO, PL, PT, RO, RS, SE, SI, SK, SM, TR)
African Intellectual Property Organization (BF, BJ, CF, CG, CI, CM, GA, GN, GQ, GW, KM, ML, MR, NE, SN, TD, TG)
Publication Language: English (EN)
Filing Language: English (EN)