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1. (WO2018031155) A MICROSCALE REACTOR AND METHODS FOR SMALL SCALE SYNTHESIS AND RAPID SCREENING CONDITIONS
Latest bibliographic data on file with the International Bureau

Pub. No.: WO/2018/031155 International Application No.: PCT/US2017/041237
Publication Date: 15.02.2018 International Filing Date: 07.07.2017
IPC:
B01J 8/00 (2006.01) ,B01J 19/00 (2006.01) ,B01L 3/00 (2006.01) ,B01L 3/08 (2006.01) ,B01L 7/00 (2006.01)
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
8
Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
19
Chemical, physical, or physico-chemical processes in general; Their relevant apparatus
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
L
CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
3
Containers or dishes for laboratory use, e.g. laboratory glassware; Droppers
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
L
CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
3
Containers or dishes for laboratory use, e.g. laboratory glassware; Droppers
08
Flasks
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
L
CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
7
Heating or cooling apparatus; Heat insulating devices
Applicants:
THE ARIZONA BOARD OF REGENTS ON BEHALF OF THE UNIVERSITY OF ARIZONA [US/US]; The University of Arizona, Tech Transfer Arizona University Services Annex, 4th Floor P.O. Box 210300A Tucson, AZ 85721, US
Inventors:
PYUN, Dong-Chul; US
PAVLOPOULOS, Nicholas, George; US
Agent:
NGUYEN, Quan; US
Priority Data:
62/373,25310.08.2016US
Title (EN) A MICROSCALE REACTOR AND METHODS FOR SMALL SCALE SYNTHESIS AND RAPID SCREENING CONDITIONS
(FR) RÉACTEUR À ÉCHELLE MICROSCOPIQUE ET PROCÉDÉS DE SYNTHÈSE À PETITE ÉCHELLE ET DE CONDITIONS DE CRIBLAGE RAPIDE
Abstract:
(EN) System and methods that provide reliable heating/cooling and mixing, coupled with uniform delivery of reagents at microscale sizes, are described herein. A microreactor vessel having one or more ports is used in a microscale reaction. Solid reagents are weighed, ground by ball milling, and added into the microreactor vessel. A particulate-filled heating mantle having a cavity configured to hold the microreactor vessel is used to heat the microreactor vessel.
(FR) L'invention porte également sur un système et sur des procédés qui permettent un chauffage/refroidissement et un mélange fiables, couplés avec une distribution uniforme de réactifs à des dimensions microscopiques. Un récipient de microréacteur ayant un ou plusieurs orifices est utilisé dans une réaction à l'échelle microscopique. Les réactifs solides sont pesés, broyés par broyage à boulets, et ajoutés dans le récipient du microréacteur. Un chauffe-ballon remplie de particules ayant une cavité configurée pour maintenir la cuve de microréacteur est utilisée pour chauffer la cuve de microréacteur.
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Designated States: AE, AG, AL, AM, AO, AT, AU, AZ, BA, BB, BG, BH, BN, BR, BW, BY, BZ, CA, CH, CL, CN, CO, CR, CU, CZ, DE, DJ, DK, DM, DO, DZ, EC, EE, EG, ES, FI, GB, GD, GE, GH, GM, GT, HN, HR, HU, ID, IL, IN, IR, IS, JO, JP, KE, KG, KH, KN, KP, KR, KW, KZ, LA, LC, LK, LR, LS, LU, LY, MA, MD, ME, MG, MK, MN, MW, MX, MY, MZ, NA, NG, NI, NO, NZ, OM, PA, PE, PG, PH, PL, PT, QA, RO, RS, RU, RW, SA, SC, SD, SE, SG, SK, SL, SM, ST, SV, SY, TH, TJ, TM, TN, TR, TT, TZ, UA, UG, US, UZ, VC, VN, ZA, ZM, ZW
African Regional Intellectual Property Organization (ARIPO) (BW, GH, GM, KE, LR, LS, MW, MZ, NA, RW, SD, SL, ST, SZ, TZ, UG, ZM, ZW)
Eurasian Patent Organization (AM, AZ, BY, KG, KZ, RU, TJ, TM)
European Patent Office (AL, AT, BE, BG, CH, CY, CZ, DE, DK, EE, ES, FI, FR, GB, GR, HR, HU, IE, IS, IT, LT, LU, LV, MC, MK, MT, NL, NO, PL, PT, RO, RS, SE, SI, SK, SM, TR)
African Intellectual Property Organization (BF, BJ, CF, CG, CI, CM, GA, GN, GQ, GW, KM, ML, MR, NE, SN, TD, TG)
Publication Language: English (EN)
Filing Language: English (EN)