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1. (WO2017135193) HYDROTREATING CATALYST FOR HYDROCARBON OIL, METHOD FOR PRODUCING HYDROTREATING CATALYST, AND HYDROTREATING METHOD
Latest bibliographic data on file with the International Bureau

Pub. No.: WO/2017/135193 International Application No.: PCT/JP2017/003197
Publication Date: 10.08.2017 International Filing Date: 30.01.2017
IPC:
B01J 27/19 (2006.01) ,B01J 21/04 (2006.01) ,B01J 32/00 (2006.01) ,B01J 35/10 (2006.01) ,B01J 37/00 (2006.01) ,B01J 37/02 (2006.01) ,B01J 37/08 (2006.01) ,C10G 45/08 (2006.01)
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
27
Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
14
Phosphorus; Compounds thereof
186
with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
188
with chromium, molybdenum, tungsten or polonium
19
Molybdenum
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
21
Catalysts comprising the elements, oxides or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium or hafnium
02
Boron or aluminium; Oxides or hydroxides thereof
04
Alumina
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
32
Catalyst carriers in general
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
35
Catalysts, in general, characterised by their form or physical properties
02
Solids
10
characterised by their surface properties or porosity
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
37
Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
37
Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
02
Impregnation, coating or precipitation
B PERFORMING OPERATIONS; TRANSPORTING
01
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
J
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS, COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
37
Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
08
Heat treatment
C CHEMISTRY; METALLURGY
10
PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
G
CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
45
Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
02
to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing
04
characterised by the catalyst used
06
containing nickel or cobalt metal, or compounds thereof
08
in combination with chromium, molybdenum, or tungsten metals, or compounds thereof
Applicants:
日揮触媒化成株式会社 JGC CATALYSTS AND CHEMICALS LTD. [JP/JP]; 神奈川県川崎市幸区堀川町580番地 580 Horikawa-cho, Saiwai-ku, Kawasaki-shi, Kanagawa 2120013, JP
Inventors:
松元 雄介 MATSUMOTO, Yusuke; JP
渡部 光徳 WATABE, Mitsunori; JP
小林 みどり KOBAYASHI, Midori; JP
Agent:
特許業務法人弥生特許事務所 YAYOY PATENT OFFICE; JP
Priority Data:
2016-01753301.02.2016JP
2016-08749925.04.2016JP
Title (EN) HYDROTREATING CATALYST FOR HYDROCARBON OIL, METHOD FOR PRODUCING HYDROTREATING CATALYST, AND HYDROTREATING METHOD
(FR) CATALYSEUR D'HYDROTRAITEMENT POUR HUILE HYDROCARBONÉE, SON PROCÉDÉ DE PRODUCTION, ET PROCÉDÉ D'HYDROTRAITEMENT
(JA) 炭化水素油の水素化処理触媒、その製造方法、および水素化処理方法
Abstract:
(EN) [Problem] To provide a hydrotreating catalyst for hydrocarbon oil, wherein the hydrotreating catalyst maintains high industrial productivity, has excellent desulfurization activity, and can regenerate a high performance catalyst. [Solution] On a γ-alumina carrier (a carrier composed of 100% γ-alumina or an inorganic composite oxide carrier obtained by mixing γ-alumina with a different metal element) are carried, for example, 15-28 parts by mass of molybdenum and/or tungsten in terms of oxides and 2-7 parts by mass of cobalt and/or nickel in terms of oxides with respect to 100 parts by mass of the catalyst, and the content of carbon derived from an organic acid is 2.0 parts by mass or less on an elemental basis. The catalyst has a specific surface area of 180-320 m2/g, and has an average pore diameter of 50-110 Å as measured by a mercury penetration method. The ignition loss of the catalyst is 5.0% or less, and the adsorption amount of nitric oxide on the sulfide-treated catalyst is 8.0 ml/g or more.
(FR) Le problème décrit par la présente invention est de produire un catalyseur d'hydrotraitement destiné à une huile hydrocarbonée, le catalyseur d'hydrotraitement maintenant une productivité industrielle élevée, possédant une excellente activité de désulfuration, et pouvant régénérer un catalyseur haute performance. La solution de l’invention porte sur un support de γ-alumine (un support composé à 100 % de γ-alumine ou un support d'oxyde composite inorganique obtenu en mélangeant de la γ-alumine avec un élément métallique différent) sur lequel sont supportés, par exemple, de 15 à 28 parties en masse de molybdène et/ou de tungstène en termes d'oxydes et de 2 à 7 parties en masse de cobalt et/ou de nickel en termes d'oxydes pour 100 parties en masse du catalyseur, et la teneur en carbone issu d'un acide organique est inférieure ou égale à 2,0 parties en masse sur une base élémentaire. Le catalyseur présente une surface spécifique de 180 à 320 m2/g, et un diamètre moyen de pore de 50 à 110 Å tel que mesuré par un procédé de pénétration du mercure. La perte par calcination du catalyseur est inférieure ou égale à 5,0 %, et la quantité d'adsorption de monoxyde d'azote sur un catalyseur traité au sulfure est supérieure ou égale à 8,0 ml/g.
(JA) 【課題】工業的に高い生産性を維持しつつ脱硫活性に優れ、高性能な触媒を再生することができる炭化水素油の水素化処理触媒を提供すること。 【解決手段】γ―アルミナ担体(γ―アルミナ100%からなる担体またはγ―アルミナに異元素金属を混合した無機複合酸化物担体)上に、触媒100質量部に対して、例えばモリブデン及び/またはタングステンが酸化物換算として15~28質量部担持され、コバルト及び/またはニッケルが酸化物換算として2~7質量部担持され、有機酸由来の炭素の含有量は、元素基準として2.0質量部以下である。また触媒の比表面積が180~320m/g、水銀圧入法で測定した平均細孔径が50~110Åである。また触媒の強熱減量が5.0%以下、硫化処理した触媒の一酸化窒素の吸着量が8.0ml/g以上である。
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Designated States: AE, AG, AL, AM, AO, AT, AU, AZ, BA, BB, BG, BH, BN, BR, BW, BY, BZ, CA, CH, CL, CN, CO, CR, CU, CZ, DE, DJ, DK, DM, DO, DZ, EC, EE, EG, ES, FI, GB, GD, GE, GH, GM, GT, HN, HR, HU, ID, IL, IN, IR, IS, KE, KG, KH, KN, KP, KR, KW, KZ, LA, LC, LK, LR, LS, LU, LY, MA, MD, ME, MG, MK, MN, MW, MX, MY, MZ, NA, NG, NI, NO, NZ, OM, PA, PE, PG, PH, PL, PT, QA, RO, RS, RU, RW, SA, SC, SD, SE, SG, SK, SL, SM, ST, SV, SY, TH, TJ, TM, TN, TR, TT, TZ, UA, UG, US, UZ, VC, VN, ZA, ZM, ZW
African Regional Intellectual Property Organization (ARIPO) (BW, GH, GM, KE, LR, LS, MW, MZ, NA, RW, SD, SL, ST, SZ, TZ, UG, ZM, ZW)
Eurasian Patent Organization (AM, AZ, BY, KG, KZ, RU, TJ, TM)
European Patent Office (AL, AT, BE, BG, CH, CY, CZ, DE, DK, EE, ES, FI, FR, GB, GR, HR, HU, IE, IS, IT, LT, LU, LV, MC, MK, MT, NL, NO, PL, PT, RO, RS, SE, SI, SK, SM, TR)
African Intellectual Property Organization (BF, BJ, CF, CG, CI, CM, GA, GN, GQ, GW, KM, ML, MR, NE, SN, TD, TG)
Publication Language: Japanese (JA)
Filing Language: Japanese (JA)
Also published as:
SG11201806008PCN108602055KR1020180111815IN201817027020