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1. WO2016140045 - SURFACTANT-CONTAINING AMIDE-COMPOUND AQUEOUS SOLUTION

Publication Number WO/2016/140045
Publication Date 09.09.2016
International Application No. PCT/JP2016/054245
International Filing Date 15.02.2016
IPC
C12P 13/02 2006.01
CCHEMISTRY; METALLURGY
12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
13Preparation of nitrogen-containing organic compounds
02Amides, e.g. chloramphenicol
C07C 231/22 2006.01
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
CACYCLIC OR CARBOCYCLIC COMPOUNDS
231Preparation of carboxylic acid amides
22Separation; Purification; Stabilisation; Use of additives
C07C 233/09 2006.01
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
CACYCLIC OR CARBOCYCLIC COMPOUNDS
233Carboxylic acid amides
01having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
02having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
09with carbon atoms of carboxamide groups bound to carbon atoms of an acyclic unsaturated carbon skeleton
C08L 33/24 2006.01
CCHEMISTRY; METALLURGY
08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
33Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Compositions of derivatives of such polymers
24Homopolymers or copolymers of amides or imides
CPC
C07C 231/22
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
CACYCLIC OR CARBOCYCLIC COMPOUNDS
231Preparation of carboxylic acid amides
22Separation; Purification; Stabilisation; Use of additives
C07C 233/09
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
CACYCLIC OR CARBOCYCLIC COMPOUNDS
233Carboxylic acid amides
01having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
02having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
09with carbon atoms of carboxamide groups bound to carbon atoms of an acyclic unsaturated carbon skeleton
C08F 120/56
CCHEMISTRY; METALLURGY
08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
120Homopolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride, ester, amide, imide or nitrile thereof
02Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
52Amides or imides
54Amides ; , e.g. N,N-dimethylacrylamide or N-isopropylacrylamide
56Acrylamide; Methacrylamide
C08F 2/28
CCHEMISTRY; METALLURGY
08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
2Processes of polymerisation
12Polymerisation in non-solvents
16Aqueous medium
22Emulsion polymerisation
24with the aid of emulsifying agents
28cationic
C12P 13/02
CCHEMISTRY; METALLURGY
12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
13Preparation of nitrogen-containing organic compounds
02Amides, e.g. chloramphenicol ; or polyamides; Imides or polyimides; Urethanes, i.e. compounds comprising N-C=O structural element or polyurethanes
Applicants
  • 三菱レイヨン株式会社 MITSUBISHI RAYON CO., LTD. [JP]/[JP]
Inventors
  • 加納 誠 KANO, Makoto
  • 萩谷 典史 HAGIYA, Norifumi
Agents
  • 田中 玲子 TANAKA, Reiko
Priority Data
2015-03981402.03.2015JP
Publication Language Japanese (JA)
Filing Language Japanese (JA)
Designated States
Title
(EN) SURFACTANT-CONTAINING AMIDE-COMPOUND AQUEOUS SOLUTION
(FR) SOLUTION AQUEUSE DE COMPOSÉ AMIDE CONTENANT UN TENSIOACTIF
(JA) 界面活性剤含有アミド化合物水溶液
Abstract
(EN)
The present invention relates to an amide-compound aqueous solution containing an amide compound and a surfactant. More specifically, the invention relates to an amide-compound aqueous solution that contains, per 1 kg of the amide compound, 2.7 to 20 mg of a cationic surfactant or, as an anionic surfactant, 0.05 to 10 mg of carboxylic acid having 15 to 20 carbons or a salt thereof. With the present invention, even in the case in which the amide compound is manufactured by using a biocatalyst, it is possible to decrease the effervescence of the amide-compound aqueous solution, and it is possible to improve the operability and yield when manufacturing an amide-compound-based polymer.
(FR)
La présente invention concerne une solution aqueuse de composé amide contenant un composé amide et un tensioactif. Plus particulièrement, l'invention concerne une solution aqueuse de composé amide qui contient, pour 1 kg du composé amide, 2,7 à 20 mg d'un tensioactif cationique ou, en tant que tensioactif anionique, 0,05 à 10 mg d'acide carboxylique comprenant 15 à 20 atomes de carbone ou un sel correspondant. Grâce à la présente invention, même dans le cas dans lequel le composé amide est fabriqué à l'aide d'un biocatalyseur, il est possible de diminuer l'effervescence de la solution aqueuse de composé amide et il est possible d'améliorer l'exploitabilité et le rendement lors de la fabrication d'un polymère à base d'un composé amide.
(JA)
 本発明は、アミド化合物と界面活性剤を含むアミド化合物水溶液に関する。より詳細には、アミド化合物1kgに対して、陽イオン界面活性剤を2.7~20mg含むか、又は陰イオン界面活性剤として炭素数15~20のカルボン酸又はその塩を0.05~10mg含むアミド化合物水溶液に関する。本発明によれば、生体触媒を用いてアミド化合物を製造する場合であっても、アミド化合物水溶液の発泡性を低減でき、アミド化合物系重合体の製造における操作性や収率を改善することができる。
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