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1. (WO2013055871) SYNTHESIS OF MSE-FRAMEWORK TYPE MOLECULAR SIEVES
Latest bibliographic data on file with the International Bureau   

Pub. No.:    WO/2013/055871    International Application No.:    PCT/US2012/059678
Publication Date: 18.04.2013 International Filing Date: 11.10.2012
IPC:
C01B 39/48 (2006.01)
Applicants: EXXONMOBIL RESEARCH AND ENGINEERING COMPANY [US/US]; 1545 Route 22 East P.O. Box 900 Annandale, NJ 08801-0900 (US)
Inventors: WESTON, Simon, Christopher; (US).
STROHMAIER, Karl, G.; (US).
VROMAN, Hilda, B.; (US)
Agent: BARRETT, Glenn, T.; Exxonmobil Research And Engineering Company 1545 Route 22 East, P.o. Box 900 Annandale, NJ 08801-0900 (US)
Priority Data:
61/546,335 12.10.2011 US
Title (EN) SYNTHESIS OF MSE-FRAMEWORK TYPE MOLECULAR SIEVES
(FR) SYNTHÈSE DE TAMIS MOLÉCULAIRES DE TYPE À STRUCTURE MSE
Abstract: front page image
(EN)A method of synthesizing a crystalline molecular sieve having an MSE framework type comprises crystallizing a reaction mixture comprising a source of water, a source of an oxide of a tetravalent element, Y, selected from at least one of silicon, tin, titanium, vanadium, and germanium, optionally a source of a trivalent element, X, a source of an alkali or alkaline earth metal, M, and a source of organic dications, Q, such as 3 -hydroxy-1-(4-(l -methylpiperidiii-1-ium-1- yl)butyl)quinuclidin-1-ium, 3-hydroxy-1-(5 -(1-methylpiperidin-1-ium-1-yl)pentyl)quinuclidin-1-ium,1, 1 '-(butane-1,4-diyi)bis(1 -methylpiperidin-1-ium), 1, 1 '-(pentane- 1,5-diyi)bis(1 -methylpiperidin-1-ium), 1, 1 '-(hexane-1,6-diyl)bis( 1 - metbylpiperidm-l -ium), and/or l,r-((3as,6a,9)-octahydropentalene-2,5-diyl)bis(l- methylpiperidm-1-ium).
(FR)L'invention concerne un procédé de synthèse d'un tamis moléculaire cristallin, ayant un type de structure MSE, qui comporte la cristallisation d'un mélange réactionnel comportant une source d'eau, une source d'un oxyde d'un élément tétravalent, Y, choisi parmi au moins l'un des éléments suivants : le silicium, l'étain, le titane, le vanadium et le germanium, éventuellement une source d'un élément trivalent, X, une source d'un métal alcalin ou alcalino-terreux, M, et une source de dications organiques, Q, tels que 3-hydroxy-1-(4-(1-méthylpipéridin-1-ium-1-yl)butyl)quinuclidin-1-ium, 3-hydroxy-1-(5-(1-méthylpipéridin-1-ium-1-yl)pentyl)quinuclidin-1-ium, 1,1'-(butane-1,4-diyl)bis(1-méthylpipéridin-1-ium), 1,1'-(pentane-1,5-diyl)bis(1-méthylpipéridin-1-ium), 1,1'-(hexane-1,6-diyl)bis(1-méthylpipéridin-1-ium), et/ou l,r-((3as,6a,9)-octahydropentalène-2,5-diyl)bis(1-méthylpipéridin-1-ium).
Designated States: AE, AG, AL, AM, AO, AT, AU, AZ, BA, BB, BG, BH, BN, BR, BW, BY, BZ, CA, CH, CL, CN, CO, CR, CU, CZ, DE, DK, DM, DO, DZ, EC, EE, EG, ES, FI, GB, GD, GE, GH, GM, GT, HN, HR, HU, ID, IL, IN, IS, JP, KE, KG, KM, KN, KP, KR, KZ, LA, LC, LK, LR, LS, LT, LU, LY, MA, MD, ME, MG, MK, MN, MW, MX, MY, MZ, NA, NG, NI, NO, NZ, OM, PA, PE, PG, PH, PL, PT, QA, RO, RS, RU, RW, SC, SD, SE, SG, SK, SL, SM, ST, SV, SY, TH, TJ, TM, TN, TR, TT, TZ, UA, UG, US, UZ, VC, VN, ZA, ZM, ZW.
African Regional Intellectual Property Organization (BW, GH, GM, KE, LR, LS, MW, MZ, NA, RW, SD, SL, SZ, TZ, UG, ZM, ZW)
Eurasian Patent Organization (AM, AZ, BY, KG, KZ, RU, TJ, TM)
European Patent Office (AL, AT, BE, BG, CH, CY, CZ, DE, DK, EE, ES, FI, FR, GB, GR, HR, HU, IE, IS, IT, LT, LU, LV, MC, MK, MT, NL, NO, PL, PT, RO, RS, SE, SI, SK, SM, TR)
African Intellectual Property Organization (BF, BJ, CF, CG, CI, CM, GA, GN, GQ, GW, ML, MR, NE, SN, TD, TG).
Publication Language: English (EN)
Filing Language: English (EN)