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1. WO2013012047 - METHOD FOR PRODUCING HYDRIDE HAVING UNSATURATED COMPOUND WITH FOUR CARBON ATOMS AS STARTING MATERIAL

Publication Number WO/2013/012047
Publication Date 24.01.2013
International Application No. PCT/JP2012/068379
International Filing Date 19.07.2012
IPC
C07C 29/17 2006.01
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
CACYCLIC OR CARBOCYCLIC COMPOUNDS
29Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
17by hydrogenation of carbon-to-carbon double or triple bonds
C07C 31/20 2006.01
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
CACYCLIC OR CARBOCYCLIC COMPOUNDS
31Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
18Polyhydroxylic acyclic alcohols
20Dihydroxylic alcohols
C07B 61/00 2006.01
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
BGENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
61Other general methods
CPC
B01J 21/08
BPERFORMING OPERATIONS; TRANSPORTING
01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
21Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
06Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
08Silica
B01J 23/44
BPERFORMING OPERATIONS; TRANSPORTING
01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
23Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
38of noble metals
40of the platinum group metals
44Palladium
B01J 23/755
BPERFORMING OPERATIONS; TRANSPORTING
01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
23Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
70of the iron group metals or copper
74Iron group metals
755Nickel
B01J 23/866
BPERFORMING OPERATIONS; TRANSPORTING
01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
23Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
70of the iron group metals or copper
76combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
84with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
85Chromium, molybdenum or tungsten
86Chromium
866Nickel and chromium
B01J 35/0006
BPERFORMING OPERATIONS; TRANSPORTING
01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
35Catalysts, in general, characterised by their form or physical properties
0006Catalysts containing parts with different compositions
B01J 35/02
BPERFORMING OPERATIONS; TRANSPORTING
01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
35Catalysts, in general, characterised by their form or physical properties
02Solids
Applicants
  • 三菱化学株式会社 MITSUBISHI CHEMICAL CORPORATION [JP]/[JP] (AllExceptUS)
  • 井澤 雄輔 IZAWA Yusuke (UsOnly)
  • 宇都宮 賢 UTSUNOMIYA Masaru (UsOnly)
  • 小西 範和 KONISHI Norikazu (UsOnly)
  • 田中 幸太 TANAKA Kouta (UsOnly)
Inventors
  • 井澤 雄輔 IZAWA Yusuke
  • 宇都宮 賢 UTSUNOMIYA Masaru
  • 小西 範和 KONISHI Norikazu
  • 田中 幸太 TANAKA Kouta
Agents
  • 濱田 百合子 HAMADA Yuriko
Priority Data
2011-15910520.07.2011JP
2011-16593728.07.2011JP
2011-24157402.11.2011JP
Publication Language Japanese (JA)
Filing Language Japanese (JA)
Designated States
Title
(EN) METHOD FOR PRODUCING HYDRIDE HAVING UNSATURATED COMPOUND WITH FOUR CARBON ATOMS AS STARTING MATERIAL
(FR) PROCÉDÉ DE PRODUCTION D'UN HYDRURE CONTENANT UN COMPOSÉ INSATURÉ AYANT QUATRE ATOMES DE CARBONE À TITRE DE MATÉRIAU DE DÉPART
(JA) 炭素原子数4の不飽和化合物を原料とする水素化物の製造方法
Abstract
(EN)
The objective of the present invention is to provide a method that is for producing a hydride having four carbon atoms and is able to reduce catalyst degradation and extend catalyst life. In a method for continuously producing a corresponding hydride having 4 carbon atoms by means of hydrogenating an unsaturated compound having four carbon atoms and in a liquid phase by causing contact with a solid catalyst obtained by supporting a metal element belonging to group 9-11 of the periodic table on a carrier, the hydrogenation is performed in the presence of 1,4-butanediol having 1 ppm to 1 wt% inclusive of a nitrogen component in terms of nitrogen atom concentration as a solvent.
(FR)
L'objet de cette invention est de pourvoir à un procédé de production d'un hydrure ayant quatre atomes de carbone et qui est capable de réduire la dégradation du catalyseur et de prolonger sa durée de vie. Dans un procédé de production en continu d'un hydrure correspondant ayant 4 atomes de carbone par hydrogénation d'un composé insaturé ayant quatre atomes de carbone et mise en contact en phase liquide avec un catalyseur solide obtenu par support d'un élément métallique appartenant aux Groupes 9 à 11 de la Classification périodique des éléments sur un support, l'hydrogénation est effectuée en présence d'un 1,4-butanediol contenant de 1 ppm à 1 % en poids inclus d'un composant azoté en termes de concentration d'atomes d'azote, à titre de solvant.
(JA)
 本発明は、触媒の劣化を軽減でき、且つ触媒寿命を延ばすことができる炭素原子数4の水素化物を製造する方法を提供することを目的とする。本発明は、炭素原子数が4の不飽和化合物を液相下で、周期表の第9~11族に属する金属元素を担体に担持させて得られる固体触媒と接触させて水素化することにより、対応する炭素原子数4の水素化物を連続的に製造する方法であって、溶媒として窒素成分が窒素原子換算の濃度で1重量ppm以上1重量%以下の1,4-ブタンジオールの存在下で水素化を行う。
Also published as
Latest bibliographic data on file with the International Bureau