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1. WO2011099351 - METHOD OF SYNTHESIZING DIAMONDOIDS, AND DIAMONDOID

Publication Number WO/2011/099351
Publication Date 18.08.2011
International Application No. PCT/JP2011/051168
International Filing Date 24.01.2011
IPC
C07C 2/00 2006.1
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
CACYCLIC OR CARBOCYCLIC COMPOUNDS
2Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms
B01J 3/00 2006.1
BPERFORMING OPERATIONS; TRANSPORTING
01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
3Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
B01J 19/08 2006.1
BPERFORMING OPERATIONS; TRANSPORTING
01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
19Chemical, physical or physico-chemical processes in general; Their relevant apparatus
08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
C07C 2/76 2006.1
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
CACYCLIC OR CARBOCYCLIC COMPOUNDS
2Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms
76by condensation of hydrocarbons with partial elimination of hydrogen
C07C 13/64 2006.1
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
CACYCLIC OR CARBOCYCLIC COMPOUNDS
13Cyclic hydrocarbons containing rings other than, or in addition to, six-membered aromatic rings
28Polycyclic hydrocarbons or acyclic hydrocarbon derivatives thereof
32with condensed rings
62with more than three condensed rings
64with a bridged ring system
C08G 61/02 2006.1
CCHEMISTRY; METALLURGY
08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
61Macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain of the macromolecule
02Macromolecular compounds containing only carbon atoms in the main chain of the macromolecule, e.g. polyxylylenes
CPC
B01J 19/088
BPERFORMING OPERATIONS; TRANSPORTING
01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
19Chemical, physical or physico-chemical processes in general; Their relevant apparatus
08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
087employing electric or magnetic energy
088giving rise to electric discharges
B01J 2219/0809
BPERFORMING OPERATIONS; TRANSPORTING
01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
2219Chemical, physical or physico-chemical processes in general; Their relevant apparatus
08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
0803employing electric or magnetic energy
0805giving rise to electric discharges
0807involving electrodes
0809employing two or more electrodes
B01J 2219/0835
BPERFORMING OPERATIONS; TRANSPORTING
01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
2219Chemical, physical or physico-chemical processes in general; Their relevant apparatus
08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
0803employing electric or magnetic energy
0805giving rise to electric discharges
0807involving electrodes
0824Details relating to the shape of the electrodes
0835substantially flat
B01J 2219/0841
BPERFORMING OPERATIONS; TRANSPORTING
01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
2219Chemical, physical or physico-chemical processes in general; Their relevant apparatus
08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
0803employing electric or magnetic energy
0805giving rise to electric discharges
0807involving electrodes
0837Details relating to the material of the electrodes
0841Metal
B01J 2219/0869
BPERFORMING OPERATIONS; TRANSPORTING
01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
2219Chemical, physical or physico-chemical processes in general; Their relevant apparatus
08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
0869Feeding or evacuating the reactor
B01J 2219/0871
BPERFORMING OPERATIONS; TRANSPORTING
01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
2219Chemical, physical or physico-chemical processes in general; Their relevant apparatus
08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
0871Heating or cooling of the reactor
Applicants
  • 国立大学法人東京大学 The University of Tokyo [JP]/[JP] (AllExceptUS)
  • 寺嶋 和夫 TERASHIMA, Kazuo [JP]/[JP] (UsOnly)
  • シュタウス スヴェン ニコ STAUSS Sven Nico [CH]/[JP] (UsOnly)
  • 宮副 裕之 MIYAZOE, Hiroyuki [JP]/[JP] (UsOnly)
  • 佐々木 岳彦 SASAKI, Takehiko [JP]/[JP] (UsOnly)
  • 菊池 宏和 KIKUCHI, Hirokazu [JP]/[JP] (UsOnly)
  • 斎藤 康也 SAITO, Koya [JP]/[JP] (UsOnly)
  • 静野 朋季 SHIZUNO, Tomoki [JP]/[JP] (UsOnly)
Inventors
  • 寺嶋 和夫 TERASHIMA, Kazuo
  • シュタウス スヴェン ニコ STAUSS Sven Nico
  • 宮副 裕之 MIYAZOE, Hiroyuki
  • 佐々木 岳彦 SASAKI, Takehiko
  • 菊池 宏和 KIKUCHI, Hirokazu
  • 斎藤 康也 SAITO, Koya
  • 静野 朋季 SHIZUNO, Tomoki
Agents
  • 牛木 護 USHIKI, Mamoru
Priority Data
2010-02928412.02.2010JP
Publication Language Japanese (ja)
Filing Language Japanese (JA)
Designated States
Title
(EN) METHOD OF SYNTHESIZING DIAMONDOIDS, AND DIAMONDOID
(FR) PROCÉDÉ DE SYNTHÈSE DE DIAMANDOÏDES, ET DIAMANDOÏDE
(JA) ダイヤモンドイドの合成方法及びダイヤモンドイド
Abstract
(EN) Disclosed is a diamondoid obtained by synthesis without utilizing catalysts and organic solvents. In a synthesis device (1), supercritical fluid or subcritical fluid with dissolved adamantane is generated in a pressure vessel (2), and plasma is generated in said supercritical fluid or subcritical fluid. By this means, the synthesis device (1) is able to generate 2nd to 15th order diamondoids of multiple bonded adamantane molecules, or the isomers of said 2nd to 15th order diamondoids. In addition to being able to synthesize lower-order diamondoids without utilizing catalysts and organic solvents, the synthesis device (1) can also obtain by synthesis higher-order diamondoids.
(FR) La présente invention concerne un diamandoïde obtenu par synthèse sans utiliser de catalyseurs ni solvants organiques. Dans un dispositif de synthèse (1), un fluide supercritique ou un fluide sous-critique avec de l'adamantane dissous est produit dans un récipient sous pression (2), et du plasma est produit dans ledit fluide supercritique ou le fluide sous-critique. De cette façon, le dispositif de synthèse (1) peut produire des diamandoïdes du 2e au 15e ordre de multiples molécules d'adamantane liées, ou les isomères desdits diamandoïdes du 2e au 15e ordre. En plus de permettre la synthèse de diamandoïdes d'ordre inférieur sans utiliser de catalyseurs ni solvants organiques, le dispositif de synthèse (1) permet également d'obtenir par synthèse des diamandoïdes d'ordre supérieur.
(JA) 触媒や有機溶媒を用いずに、合成により得られるダイヤモンドイドを提供できるようにすることを目的とする。 合成装置1では、アダマンタンを溶解させた超臨界流体又は亜臨界流体を耐圧容器2内に生成し、当該超臨界流体中又は亜臨界流体中にプラズマを発生させる。これにより合成装置1では、複数のアダマンタンを結合させた2次~15次ダイヤモンドイド、これら2次~15次ダイヤモンドイドの各異性体を生成でき、触媒や有機溶媒を用いずに低次ダイヤモンドイドを合成できると共に、高次ダイヤモンドイドについても合成により得ることができる。
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