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1. (WO2009139973) MICROWAVE-ASSISTED SYNTHESIS OF PERFLUOROPHTHALOCYANINE MOLECULES
Latest bibliographic data on file with the International Bureau   

Pub. No.:    WO/2009/139973    International Application No.:    PCT/US2009/039068
Publication Date: 19.11.2009 International Filing Date: 01.04.2009
IPC:
C09B 47/04 (2006.01)
Applicants: NEW JERSEY INSTITUTE OF TECHNOLOGY [US/US]; 323 Martin Luther King, Jr. Boulevard Office Of The Research And Development Newark, NJ 07102-1982 (US) (For All Designated States Except US).
FRAUNHOFER-GESELLSCHAFT ZUR FOERDERUNG DER ANGEWANDTEN FORSCHUNG E.V. [DE/DE]; Hansastrasse 27c 86086 Muenchen (DE) (For All Designated States Except US).
GORUN, Sergiu, M. [US/US]; (US) (For US Only).
SCHNURPFEIL, Guenter [DE/DE]; (DE) (For US Only).
HILD, Olaf [DE/DE]; (DE) (For US Only).
WOEHRLE, Dieter [DE/DE]; (DE) (For US Only).
TSARYOVA, Olga [DE/DE]; (DE) (For US Only).
GERDES, Robert [US/US]; (US) (For US Only)
Inventors: GORUN, Sergiu, M.; (US).
SCHNURPFEIL, Guenter; (DE).
HILD, Olaf; (DE).
WOEHRLE, Dieter; (DE).
TSARYOVA, Olga; (DE).
GERDES, Robert; (US)
Agent: NABULSI, Basam E; McCarter & English, LLP Canterbury Green 201 Broad Street, 9th Floor Stamford, CT 06901 (US)
Priority Data:
61/118,830 01.12.2008 US
61/072,571 01.04.2008 US
Title (EN) MICROWAVE-ASSISTED SYNTHESIS OF PERFLUOROPHTHALOCYANINE MOLECULES
(FR) SYNTHÈSE ASSISTÉE PAR MICRO-ONDES DE MOLÉCULES DE PERFLUOROPHTHALOCYANINE
Abstract: front page image
(EN)Advantageous microwave-assisted methods for synthesis of fluorinated phthalocyanines are provided. The microwave-assisted methods offer enhanced yields, substantially eliminate reaction solvents, and facilitate purification relative to conventional synthesis techniques. Typical implementation involve a reaction mixture that includes perfluoro-phthalonitrile that is reacted in a vessel with application of microwave energy for a reaction period sufficient to yield a fluorinated phthalocyanine. The fluorinated phthalocyanines synthesized according to the disclosed microwave-assisted methods have wide ranging applications, e.g., corrosion-related applications, coating-related applications, catalysis, and the production of optical and electronic materials.
(FR)L'invention concerne des procédés avantageux assistés par micro-ondes avantageux pour la synthèse de phthalocyanines fluorées. Les procédés assistés par micro-ondes procurent des rendements améliorés, éliminent sensiblement les solvants de réaction et facilitent la purification par rapport aux techniques de synthèse conventionnelles. Une mise en oeuvreœuvre type implique un mélange de réaction qui comprend du perfluoro-phthalonitrile que l'on fait réagir dans une cuve avec l'application de micro-ondes pendant un temps de réaction suffisant pour produire de la phthalocyanine fluorée. Les phthalocyanines fluorées synthétisées selon les procédés assistés par micro-ondes décrits trouvent une large gamme d'applications, par exemple, des applications liées à la corrosion, des applications liées à des opérations de revêtement, la catalyse et la production de matériaux optiques et électroniques.
Designated States: AE, AG, AL, AM, AO, AT, AU, AZ, BA, BB, BG, BH, BR, BW, BY, BZ, CA, CH, CN, CO, CR, CU, CZ, DE, DK, DM, DO, DZ, EC, EE, EG, ES, FI, GB, GD, GE, GH, GM, GT, HN, HR, HU, ID, IL, IN, IS, JP, KE, KG, KM, KN, KP, KR, KZ, LA, LC, LK, LR, LS, LT, LU, LY, MA, MD, ME, MG, MK, MN, MW, MX, MY, MZ, NA, NG, NI, NO, NZ, OM, PG, PH, PL, PT, RO, RS, RU, SC, SD, SE, SG, SK, SL, SM, ST, SV, SY, TJ, TM, TN, TR, TT, TZ, UA, UG, US, UZ, VC, VN, ZA, ZM, ZW.
African Regional Intellectual Property Organization (BW, GH, GM, KE, LS, MW, MZ, NA, SD, SL, SZ, TZ, UG, ZM, ZW)
Eurasian Patent Organization (AM, AZ, BY, KG, KZ, MD, RU, TJ, TM)
European Patent Office (AT, BE, BG, CH, CY, CZ, DE, DK, EE, ES, FI, FR, GB, GR, HR, HU, IE, IS, IT, LT, LU, LV, MC, MK, MT, NL, NO, PL, PT, RO, SE, SI, SK, TR)
African Intellectual Property Organization (BF, BJ, CF, CG, CI, CM, GA, GN, GQ, GW, ML, MR, NE, SN, TD, TG).
Publication Language: English (EN)
Filing Language: English (EN)