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1. WO2002006209 - SYNTHESIS METHOD FOR N1,N3-BIS (2.AMINOETHYL) PROPANE-1,3-DIAMINE, SYNTHESIS INTERMEDIATES, RESULTING PRODUCTS AND USE THEREOF IN SYNTHESIS OF CYCLAM

Publication Number WO/2002/006209
Publication Date 24.01.2002
International Application No. PCT/FR2001/002293
International Filing Date 16.07.2001
Chapter 2 Demand Filed 12.12.2001
IPC
C07C 209/62 2006.1
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
CACYCLIC OR CARBOCYCLIC COMPOUNDS
209Preparation of compounds containing amino groups bound to a carbon skeleton
62by cleaving carbon-to-nitrogen, sulfur-to-nitrogen, or phosphorus-to-nitrogen bonds, e.g. hydrolysis of amides, N-dealkylation of amines or quaternary ammonium compounds
C07C 211/14 2006.1
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
CACYCLIC OR CARBOCYCLIC COMPOUNDS
211Compounds containing amino groups bound to a carbon skeleton
01having amino groups bound to acyclic carbon atoms
02of an acyclic saturated carbon skeleton
14Amines containing amino groups bound to at least two aminoalkyl groups, e.g. diethylenetriamines
C07D 403/14 2006.1
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
DHETEROCYCLIC COMPOUNDS
403Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, not provided for by group C07D401/167
14containing three or more hetero rings
CPC
C07C 209/62
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
CACYCLIC OR CARBOCYCLIC COMPOUNDS
209Preparation of compounds containing amino groups bound to a carbon skeleton
62by cleaving carbon-to-nitrogen, sulfur-to-nitrogen, or phosphorus-to-nitrogen bonds, e.g. hydrolysis of amides, N-dealkylation of amines or quaternary ammonium compounds
C07C 211/14
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
CACYCLIC OR CARBOCYCLIC COMPOUNDS
211Compounds containing amino groups bound to a carbon skeleton
01having amino groups bound to acyclic carbon atoms
02of an acyclic saturated carbon skeleton
14Amines containing amino groups bound to at least two aminoalkyl groups, e.g. diethylenetriamines
C07D 403/14
CCHEMISTRY; METALLURGY
07ORGANIC CHEMISTRY
DHETEROCYCLIC COMPOUNDS
403Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, not provided for by group C07D401/00
14containing three or more hetero rings
Applicants
  • UNIVERSITE DE BRETAGNE OCCIDENTALE [FR]/[FR] (AllExceptUS)
  • HANDEL, Henri [FR]/[FR] (UsOnly)
  • BERNARD, Hélène [FR]/[FR] (UsOnly)
  • ANTOINE, Marine [FR]/[FR] (UsOnly)
Inventors
  • HANDEL, Henri
  • BERNARD, Hélène
  • ANTOINE, Marine
Agents
  • POUPON, Michel
Priority Data
00/0956919.07.2000FR
Publication Language French (fr)
Filing Language French (FR)
Designated States
Title
(EN) SYNTHESIS METHOD FOR N1,N3-BIS (2.AMINOETHYL) PROPANE-1,3-DIAMINE, SYNTHESIS INTERMEDIATES, RESULTING PRODUCTS AND USE THEREOF IN SYNTHESIS OF CYCLAM
(FR) PROCEDE DE SYNTHESE DE LA N1, N3-BIS (2-AMINOETHYL)PROPANE-1,3-DIAMINE, INTERMEDIAIRES DE SYNTHESE, PRODUITS AINSI OBTENUS ET LEUR APPLICATION A LA SYNTHESE DE CYCLAM
Abstract
(EN) The invention concerns a method of synthesis of a linear polynitrogen-containing derivative, namely N1,N3-bis (2-aminoethyl) propane-1,3-diamine of general formula (I) using as synthesis intermediates compounds (II) and (III). The invention also concerns the resulting products and their use in the synthesis of cyclic polynitrogen-containing derivatives such as cyclam.
(FR) L'invention a pour objet un procédé de synthèse d'un dérivé polyazoté linéaire à savoir la N1,N3-bis (2-aminoéthyl) propane-1,3-diamine, de formule générale (I): (I) faisant intervenir comme intermédiaires de synthèse les composés (II) et (III) Elle concerne également les produits ainsi obtenus et leur application à la synthèse de dérivés polyazotés cycliques tels que le cyclam.
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